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Identity and purity verified by High-Performance Liquid Chromatography with UV Detection coupled with Mass Spectrometry (HPLC-UV/MS)
For the standalone overview, see The Wolverine Stack Explained
The organic layers from two extractions were combined and aliquots were analyzed on a 4000 Q-Trap mass spectrometer (AB SCIEX, Framingham, MA) using the 50 2.1 mm Hydrophilic Interaction Liquid Chromatography (HILIC-LC) column (Waters Corp., Milford, MA)
J.BergerS
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