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It was randomized, meaning allocation to dose groups was random

Brissova M, Shiota M, Nicholson WE, Gannon M, Knobel SM, Piston DW, Wright CV, Powers AC

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The final isolation, amino acid analysis, sequence and synthesis, and the delta EEG (sleep)- --inducing properties of the synthetic compound were first reported in 1976-1978

10.1167/tvst.7.3.1 Mynarczyk M, Falkowska M, Micun Z, Obuchowska I, Kochanowicz J, Socha K, Konopiska J: Diet, Oxidative Stress, and Blood Serum Nutrients in Various Types of Glaucoma: A Systematic Review

The article names five: inability to eat solid food for more than one day, dehydration despite fluid intake, blood glucose consistently below 70 mg/dL, acute abdominal pain radiating to the back, and elevated lipase on lab work